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2026, 05, v.32 13-22
基于干法制粒的玫瑰香基颗粒在加热卷烟滤嘴中的香气释放特征及评价
基金项目(Foundation): 江苏中烟工业有限责任公司科技项目“基于咖啡渣内源大分子颗粒的载香功能评价与应用研究”(202606); 中国烟草总公司科技项目“超低焦中式烤烟型卷烟设计技术体系构建与应用”(Y022202401)
邮箱(Email): zhulj@jszygs.com;
DOI: 10.16472/j.chinatobacco.2026.T0067
发布时间: 2026-07-29
出版时间: 2026-07-29
网络发布时间: 2026-07-29
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摘要:

【目的】掌握玫瑰香基颗粒在加热卷烟滤嘴中的香气释放特征。【方法】以玫瑰粉末、乳糖和糊精作为原料,采用干法制粒工艺制备不同原料配比的玫瑰香基颗粒,使用顶空-气相质谱(HS-GC/MS)在特定温度下考察玫瑰香基颗粒的香气释放特征,并对添加应用后的加热卷烟进行抽吸感官评价。【结果】(1)6个产地玫瑰香基颗粒共鉴定出30种挥发性成分,其中平阴玫瑰有18种、苦水玫瑰有17种、和田玫瑰有14种、墨红玫瑰有15种、保加利亚玫瑰有15种、法国玫瑰有22种,共有的挥发性成分有7种,其中苯乙醇含量占比最高,为42.2%~78.8%。(2)不同原料配比玫瑰香基颗粒的香气释放特征不同,随着乳糖含量的降低,糊精含量的增加,玫瑰香基颗粒的主要挥发成分总质量先逐渐降低,后缓慢增加。(3)不同原料配比对玫瑰香基颗粒的堆密度和孔体积均有影响,当玫瑰粉末、乳糖和糊精的配比为5:2:3时,玫瑰香基颗粒在加热卷烟中的协调性和一致性好,感官评价最高。

Abstract:

[Objective] This study aimed to characterize the aroma released from rose-based granules in heated-tobacco-product filters. [Methods] Rose powder, lactose, and dextrin were used to prepare rose-based granules with different ingredient ratios by dry granulation. Aroma-release characteristics were investigated at specified temperatures using headspace gas chromatography-mass spectrometry(HS-GC/MS), and heated tobacco products containing the granules were evaluated by sensory analysis. [Results](1) A total of 30 volatile compounds were identified in rose-based granules prepared from roses originating in six regions: 18 in Pingyin roses, 17 in Kushui roses, 14 in Hotan roses, 15 in Mohong roses, 15 in Bulgarian roses, and 22 in French roses. Seven volatile compounds were common to all granules, among which phenethyl alcohol had the highest relative content(42.2%-78.8%).(2) The aroma-release characteristics varied with the ingredient ratio. As the lactose content decreased and the dextrin content increased, the total mass of the major volatile compounds initially decreased and then increased slowly.(3) Ingredient ratios affected both the bulk density and pore volume of the granules. At a rose powder:lactose:dextrin ratio of 5:2:3, the granules exhibited good harmony and consistency in heated tobacco products and achieved the highest sensory-evaluation score. [Conclusion] Rose-based granules prepared by dry granulation retained the characteristic aroma of roses and exhibited favorable aroma-release properties in heated-tobacco-product filters. The ingredient ratio of 5:2:3 provided the best overall performance.

参考文献

[1]贾学伟,代玉祥,崔春,等.甘草固体颗粒香料的改良及卷烟加香应用[J].中国烟草学报, 2025, 31(1):30-39.JIA Xuewei, DAI Yuxiang, CUI Chun, et al. Improvement of licorice solid granular spice and its application in cigarette flavoring[J]. Acta Tabacaria Sinica, 2025, 31(1):30-39.

[2]尤晓娟,何红梅,刘献军,等.基于静态顶空–GC/MS的加热卷烟用滤嘴载香颗粒评价研究[J].中国烟草学报,2022, 28(1):8-16.YOU Xiaojuan, HE Hongmei, LIU Xianjun, et al. Evaluation of flavored granules in electrical heated cigarette filters based on static headspace GC/MS method[J]. Acta Tabacaria Sinica, 2022,28(1):8-16.

[3]杨屹,段勤,杨雪燕,等.热裂解–气相色谱–质谱法分析烟用咖啡颗粒热裂解特性[J].化学分析计量,2023, 32(8):70-74.YANG Yi, DUAN Qin, YANG Xueyan, et al. Analysis for pyrolysis characteristics of tobacco coffee granules by Py-GCMS[J]. Chemical Analysis and Meterage, 2023, 32(8):70-74.

[4]凌孝存,张亮,周枫,等.奶香颗粒制备及其在细支三元空腔活性炭滤嘴卷烟中的应用[J].湖南文理学院学报(自然科学版),2022, 34(4):57-64, 92.LIN Xiaocun, ZHANG Liang, ZHOU Feng, et al. Structural optimization of a milk fragrance particle and its application in fine-branched ternary cavity activated carbon filter rod cigarettes[J].Journal of Hunan University of Arts and Science(Science and Technology), 2022, 34(4):57-64, 92.

[5]朱亚峰,胡军,唐荣成,等.卷烟滤嘴加香研究进展[J].中国烟草学报,2011, 17(6):104-109.ZHU Yafeng, HU Jun, TANG Rongcheng, et al. Recent advances in research and development in cigarette filter flavoring technique[J].Acta Tabacaria Sinica, 2011, 17(6):104-109.

[6]李范珠,狄留庆.中药药剂学[M].北京:人民卫生出版社,2022:219-223.LI Fanzhu, DI Liuqing. Chinese Pharmaceutics[M]. Beijing:People's Medical Publishing House, 2022:219-223.

[7]方亮.药剂学[M].北京:人民卫生出版社,2023:231-236.FANG Liang. Pharmaceutics[M]. Beijing:People's Medical Publishing House, 2023:231-236.

[8]贾学伟,代玉祥,何峰,等.薄荷颗粒香料的干燥工艺及滤棒加香应用研究[J].轻工学报,2024 , 39(3):62-71.JIA Xuewei, DAI Yuxiang, HE Feng, et al. Drying process of peppermint granular spices and its application in flavoring filter rod[J]. Journal of Light Industry, 2024, 39(3):62-71.

[9]张晓旭,万宇超,李园园,等.不同提取工艺制备的果干复合香料化学成分与致香效果分析[J].轻工学报,2020, 35(4), 46-53.ZHANG Xiaoxu, WAN Yuchao, LI Yuanyuan, et al. Analysis of chemical composition and aroma effect of dried fruit compound spices extracted by different process[J]. Journal of Light Industry,2020, 35(4), 46-53.

[10]况弯弯,伍振峰,万娜,等.中药干法制粒的研究思路探讨:基于干法制粒技术研究的国内外研究进展[J].中国中药杂志,2019, 44(15):3195-3202.KUANG Wanwan, WU Zhenfeng, WAN Na, et al. Discussion on research thought of dry granulation of traditional Chinese medicine:research progress at home and abroad based on dry granulation technology[J]. China Journal of Chinese Materia Medica, 2019,44(15):3195-3202.

[11]程佩佩,翟红伟,赵玉婷,等.加味玉屏风颗粒干法制粒工艺的优化[J].中国医药工业杂志,2023, 54(2):237-242, 253.CHENG Peipei, ZHAI Hongwei, ZHAO Yuting, et al. Optimization of dry granulation technology of modified yupingfeng granules[J].Chinese Journal of Pharmaceuticals, 2023, 54(2):237–242, 253.

[12]史辞辞,赵月璇,赵梓先,等.热炎宁颗粒干法制粒工艺优化及物理指纹图谱研究[J].世界中医药,2025, 20(14):2441-2447.SHI Cici, ZHAO Yuexuan, ZHAO Zixian, et al. Dry granulation process optimization and physical fingerprint of reyanning granules[J]. World Chinese Medicine, 2025, 20(14):2441-2447.

[13]王坤,姚彬彬,王胜晓,等.滤棒加香技术研究进展[J].精细化工中间体,2023, 53(5):12-16.WANG Kun, YAO Binbin, WANG Shengxiao, et al. Progress in the technology of flavoring cigarette filter[J]. Fine Chemical Intermediates, 2023, 53(5):12-16.

[14]韩云辉.烟用材料生产技术及应用[M].北京:中国标准出版社,2012:44-51.HAN Yunhui. Production technology and application of tobacco materials[M]. Beijing:Standards Press of China, 2012:44-51.

[15]吴酉芝,李保国,应月.阿拉伯胶对滤棒薄荷香精微胶囊缓释性能的影响[J].食品工业科技,2010, 31(7):304-307.WU Youzhi, LI Baoguo, YING Yue. Effect of Arabic Gum on Release Performance of Filter Mint Flavor Microcapsules[J].Science and Technology of Food Industry, 2010, 31(7):304-307.

[16]郭新月,杨占平,宋晓梅,等.加热不燃烧卷烟烟气降温技术研究进展[J].中国烟草学报,2020, 26(3):24-32.GUO Xinyue, YANG Zhanping, SONG Xiaomei, et al. Research progress of cooling technology of heat-not-burn cigarette smoke[J].Acta Tabacaria Sinica, 2020, 26(3):24-32.

[17]刘显军,王颖,王冲,等.不同构型滤嘴卷烟的温度变化规律研究[J].轻工科技,2023, 39(3):27-29.LIU Xianjun, WANG Ying, WANG Chong, et al. Research on the temperature variation patterns of cigarettes with different filter configurations[J]. Light Industry Science and Technology, 2023,39(3):27-29.

[18]孔浩辉,李宏伟,卢志菁,等.卷烟滤嘴设计对主流烟气温度的影响及其降温效应[J].烟草科技,2021, 54(7):89-96.KONG Haohui, LI Hongwei, LU Zhijing, et al. Influences of cigarette filter designs on mainstream smoke temperature and cooling effect of filler[J]. Tobacco Science&Technology, 2021,54(7):89-96.

[19]MAJUMDAR R, ALEXANDER K S, RIGA A T. Physical characterization of polyethylene glycols by thermal analytical technique and the effect of humidity and molecular weight[J]. Die Pharmazie, 2010, 65(5):343-347.

[20]刘雯,余玉梅,王道铨,等.基于滤嘴抽吸温度的载香凝胶滤棒开发与应用[J].烟草科技,2022, 55(6):71-79.LIU Wen, YU Yumei, WANG Daoquan, et al. Development and application of flavoring gel filter rod based on filter temperature during puffing[J].Tobacco Science&Technology, 2022, 55(6):71-79.

[21]杜玲玲,孟晓伟,胡伊涵,等.不同陈化年份陈皮(樟头红)挥发成分差异的电子鼻与HS-GC-MS对比分析[J].食品科学,2025, 46(11):253-262.DU Lingling, MENG Xiaowei, HU Yihan, et al. Integration of electronic nose and headspace gas chromatography-mass spectrometry for differentiating the volatile compositions of citri reticulatae pericarpium made from citrus reticulata blanco var.zhany shuensis f. aged for different years[J]. Food Science,2025, 46(11):253-262.

[22]辛力,温佳文,龚文慧,等.基于HS–GC–MS及智能感官技术分析赤石脂炒陈皮炮制前后的挥发性成分差异[J].中国实验方剂学杂志,2025, 31(7):157-162.XIN Li, WEN Jiawen, GONG Wenhui, et al. Analysis of Volatile Components in Calcined Red Peony Root Before and After Processing Using HS-GC-MS and Intelligent Sensory Technology[J]. Chinese Journal of Experimental Formulary, 2025, 31(7):157-162.

[23]王蔚,黄旭建,易国春,等. HS-GC/MS法分析乌龙茶挥发性成分[J].天然产物研究与开发,2019, 31(2):222-229.WANG Wei, HUANG Xujian, YI Guochun, et al. Analysis of volatile components in Oolong tea by HS-GC/MS[J]. Natural Product Research and Development , 2019, 31(2):222-229.

[24]FEI C H, XUE Q Q, LI W J, et al Variations in volatile flavour compounds in Crataegi fructus roasting revealed by E-nose and HS-GC-MS[J]. Frontiers in Nutrition, 2023,(9):1035623.

[25]郑郁清,彭嘉玉,郭静英,等.顶空气相色谱–质谱法结合相对气味活度值法分析谷糠、麦麸、蜜糠、蜜麸4种辅料的风味成分[J].中草药,2024, 55(13):4361-4372.ZHENG Yuqing, PENG Jiayu, GUO Jingying, et al. HS-GC-MS combined with relative odor activity value method to analyze flavor components of four excipients:chaff, bran, honey chaff and honey bran[J]. Chinese Traditional and Herbal Drugs, 2024, 55(13):4361-4372.

[26]DING Y M, GUO X H, YANG J B, et al. Study on authenticity identification and quality evaluation of Styrax by combining multiple detection methods with scientific characterization of description[J]. Food Research International, 2025, 208:116217.

[27]谢建平.烟草香原料[M].北京:化学工业出版社,2009:129.XIE Jianping. Tobacco perfume materials[M]. Beijing:Chemical Industry Press, 2009:129.

基本信息:

DOI:10.16472/j.chinatobacco.2026.T0067

中图分类号:TS452;O657.63

引用信息:

[1]李炜,朱怀远,王珂清,等.基于干法制粒的玫瑰香基颗粒在加热卷烟滤嘴中的香气释放特征及评价[J].中国烟草学报,2026,32(05):13-22.DOI:10.16472/j.chinatobacco.2026.T0067.

基金信息:

江苏中烟工业有限责任公司科技项目“基于咖啡渣内源大分子颗粒的载香功能评价与应用研究”(202606); 中国烟草总公司科技项目“超低焦中式烤烟型卷烟设计技术体系构建与应用”(Y022202401)

发布时间:

2026-07-29

出版时间:

2026-07-29

网络发布时间:

2026-07-29

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